Metrological and operational characteristics of the multichannel vacuum atomic-emission spectrometer for educational and industrial laboratories with a MS-200UN spark generator

Authors

  • Vladimir M. Bychkov Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus
  • Yaroslav I. Didkovsky Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus
  • Maksim N. Kovalenko Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus
  • Anatoli A. Minko Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus
  • Mikhail R. Pasliadovich Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus
  • Sergei N. Sharashkin Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus
  • Vera M. Yakavets Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus

Keywords:

vacuum atomic-emission spectrometer, spark generator, spectral analysis, spectroscopy, multielement  semiconductor photodetectors, CCD

Abstract

This work presents the metrological and operational characteristics of the multichannel vacuum atomic-emission spectrometer for educational and industrial laboratories with a MS-200UN spark generator. The spectrometer uses an original optical scheme consisting of two polychromators: the first polychromator is designed to work in the field of vacuum ultraviolet at the wavelength range from 170 to 290 nm; the second polychromator covers the wavelength range from 290 to 410 nm. The multielement semiconductor photodetectors with remote shielding windows offer fast recording of spectra in the vacuum ultraviolet range for simultaneous evaluation of the concentrations of several chemical elements in the samples under study. It is demonstrated that metrological characteristics of the atomic-emission vacuum spectrometer with a MS-200UN spark generator for educational and industrial laboratories meet the requirements of the normative documents standardizing analysis of metals and alloys. The designed spectrometer may be used in educational process and during routine analyses at laboratories of industrial enterprises and other organizations.

Author Biographies

  • Vladimir M. Bychkov, Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus

    head of the training laboratory, department of nuclear physics, faculty of physics

  • Yaroslav I. Didkovsky, Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus

    senior researcher at the laboratory of spectroscopic systems, department of physical optics and applied informatics, faculty of physics

  • Maksim N. Kovalenko, Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus

    head of the laboratory of spectroscopic systems, department of physical optics and applied informatics, faculty of physics

  • Anatoli A. Minko, Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus

    doctor of science (physics and mathematics), full professor; head of the department of physical optics and applied informatics, faculty of physics

  • Mikhail R. Pasliadovich, Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus

    PhD (physics and mathematics), docent; leading engineer at the department of physical optics and applied informatics, faculty of physics

  • Sergei N. Sharashkin, Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus

    senior researcher at the laboratory of spectroscopic systems, department of physical optics and applied informatics, faculty of physics

  • Vera M. Yakavets, Belarusian State University, 4 Niezaliežnasci Avenue, Minsk 220030, Belarus

    optical and laser equipment engineer at the department of physical optics and applied informatics, faculty of physics

References

  1. Landsberg GS. Optika [Optics]. Moscow: Fizmatlit; 2003. 848 p. Russian.
  2. Voropay ES, Ermalitskaya KF, Zazhogin AP, Patapovich MP, Fadaiyan AR. Atomic emission multichannel spectral analysis: scientific and practical application. Vestnik BGU. Seriya 1. Fizika. Matematika. Informatika. 2009;1:4 –14. Russian.
  3. Seidel AN. Osnovy spektral’nogo analiza [Fundamentals of spectral analysis]. Moscow: Nauka; 1965. Russian.
  4. Kovalenko MN, Chekan VA, Markova LV, Koleda VV, Turutin AF. [Analytical control in the metallurgical industry]. Lit’e i metallurgiya. 2001;(4):127–130. Russian.
  5. Didkovskiy YI, Kovalenko MN, Minko AA, Posledovich MR. Multichannel atomic emission spectrometer with a spark generator. Vestnik BGU. Seriya 1. Fizika. Matematika. Informatika. 2015;1:21–25. Russian.
  6. Didkovskiy YI, Kovalenko MN, Minko AA, Posledovich MR. [Programmable spectrum excitation source for atomic emission spectral analysis]. In: Priborostroenie-2012. Materialy 5-i Mezhdunarodnoi nauchno-tekhnicheskoi konferentsii; 21–23 noyabrya 2012 g.; Minsk, Belarus’ [Instrumentation-2012. Materials of the 5th International scientific and technical conference; 2012 November 21–23; Minsk, Belarus. Minsk: Belarusian National Technical University; 2012. p. 61– 63. Russian.
  7. Minko AA, Bychkov VM, Mihalevich VF. PMA MN 2488 –2015. Multichannel atomic emission spectrometer for educational and industrial laboratories with a CLR spark generator MS-200UN. The program and methodology for metrological certification. Minsk: Institute of Metrology; 2015. Russian.
  8. National Institute of Standards and Technology (NIST). Atomic Spectra Database [Internet, cited 2018 August 22]. Available from: https://www.nist.gov/pml/atomic-spectra-database.
  9. GOST 27809 – 95. Cast iron and steel. Methods of spectrographic analysis. Moscow: Izdatel’stvo standartov «IPK»; 1996. Russian.
  10. Institut standartnykh obraztsov. Dlya spektral’nogo analiza. Stali, UG [Internet]. Yekaterinburg [cited 2019 May 12]. Available from: http://icrm-ekb.ru/catalog/data/g783d94.html. Russian.

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Published

2019-10-03

How to Cite

(1)
Bychkov, V. M. .; Didkovsky, Y. I. .; Kovalenko, M. N.; Minko, A. A.; Pasliadovich, M. R. .; Sharashkin, S. N. .; Yakavets, V. M. . Metrological and Operational Characteristics of the Multichannel Vacuum Atomic-Emission Spectrometer for Educational and Industrial Laboratories With a MS-200UN Spark Generator. Журнал Белорусского государственного университета. Физика 2019, No. 3, 51-60. https://doi.org/10.33581/2520-2243-2019-3-51-60.